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2004
Hydroxylation
O 0216
Sodium Chlorite as an Efficient Oxidant and Hydroxy Ion Pump in Osmium-CatAsymmetric Dihydroxylation. — Sodium chlorite is successfully applied as
45- 044 alyzed
reoxidant in the asymmetric Sharpless dihydroxylation of various olefins, including terminal or internal aliphatic or aromatic olefins. The reaction provides the diols in enantioselectivities comparable to the previously presented K3[Fe(CN)6] reoxidant. NaClO2
also provides the dihydroxylation process with the stoichiometric number of hydroxide
ions. — (JUNTTILA, M. H.; HORMI*, O. E. O.; J. Org. Chem. 69 (2004) 14,
4816-4820; Dep. Chem., Univ. Oulu, SF-90570 Oulu, Finland; Eng.) — Mischke
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