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2004
Antibiotics
U 1200
45- 236
Two Approaches to the Synthesis of the Macrodiolide Colletotriene. — Two convergent syntheses are developed for the synthesis of title compound (V), which may be
readily adapted for the selective incorporation of deuterium at various positions to give
access to substrates required for biosynthetic studies. The second approach is accompanied by some unexpected E/Z-isomerization of the vinyl stannane double bond to
give the by-product (XI). — (MUNOZ, D. M.; PASSEY, S. C.; SIMPSON, T. J.;
WILLIS*, C. L.; CAMPBELL, J. B.; ROSSER, R.; Aust. J. Chem. 57 (2004) 7,
645-649; Sch. Chem., Univ. Bristol, Cantock's Close, Bristol BS8 1TS, UK; Eng.) —
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