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2004
Addition reactions
O 0060
(PCy3)2Cl 2Ru=CHPh Catalyzed Kharasch Additions. Application in a Formal
Carbonylation. — The addition of trichloroalkanes to styrenes and acrylic acid
46- 035 Olefin
ester in the presence of Grubbs' catalyst provides trihalogenated products. Upon hydrolysis, they are converted into α,β-unsaturated ketones, aldehydes or γ-hydroxybutenolides. This two-step process represents an overall acylation or carbonylation of
the starting olefin. — (LEE, B. T.; SCHRADER, T. O.; MARTIN-MATUTE, B.;
KAUFFMAN, C. R.; ZHANG, P.; SNAPPER*, M. L.; Tetrahedron 60 (2004) 34,
7391-7396; Dep. Chem., Merkert Chem. Cent., Boston Coll., Chestnut Hill,
MA 02467, USA; Eng.) — Klein
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