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2004
Dehalogenation
O 0236
Pd/C-Catalyzed Transfer Reduction of Aryl Chlorides with Sodium Formate in
— The reaction of aryl chlorides (I) with sodium formate under the action of
46- 049 Water.
Pd—C under mild conditions affords the dehalogenated products (II) in good to excellent yields. It is shown, however, that an additional reduction of the aromatic to alicyclic
rings can be achieved at higher temperatures, although this process is not complete for
all substrates [cf. (V), (VI)]. — (ARCADI*, A.; CERICHELLI, G.; CHIARINI, M.;
VICO, R.; ZORZAN, D.; Eur. J. Org. Chem. 2004, 16, 3404-3407; Dip. Chim. Ing.
Chim. Mater., Univ. L'Aquila, Coppito, I-67010 L'Aquila, Italy; Eng.) — Mischke
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