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2004
Polyphenyl derivatives
Q 0700
A Fluorous-Tagged, Acid-Labile Protecting Group for the Synthesis of Carboxand Sulfonamides. — The preparation of a 27-member library of biaryl sul46- 090 amides
fonamides and a 18-member library of biaryl carboxamides is based on the initial reductive amination of aldehyde (II) with amines of type (I) or (IX). Intermediates are
purified by solid-phase extraction over reversed-phase fluorous silica gel to afford the
target compounds in high yields and purities without the need for column chromatographic purification. — (VILLARD, A.-L.; WARRINGTON, B. H.; LADLOW*, M.;
J. Comb. Chem. 6 (2004) 4, 611-622; GSK Cambridge Technol. Cent., Univ. Chem.
Lab., Cambridge CB2 1EW, UK; Eng.) — Klein
2004
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