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2004
Oxidation
O 0212
48- 040
Palladium-Catalyzed Oxygenation of Unactivated sp3 C—H Bonds. — The new
method using Ph-I(OAc)2 as a stoichiometric oxidant is applicable to a variety of substrates. Mono-β-oxygenated products are obtained as a mixture of E/Z isomers. Reactivity toward oxidation is enhanced by α-branching as is shown in the first example.
No reaction is observed for substrates (IV). — (DESAI, L. V.; HULL, K. L.;
SANFORD*, M. S.; J. Am. Chem. Soc. 126 (2004) 31, 9542-9543; Dep. Chem.,
Univ. Mich., Ann Arbor, MI 48109, USA; Eng.) — Adam
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