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2004
Zinc
I 1700
50- 017
A New 3-D Open-Framework Zinc Phosphate [C6H16 N2]·[Zn2(HPO4)3] Synthesized by a Solvothermal Combinatorial Approach. — The title compound is
synthesized solvothermally by a combinatorial approach from mixtures of
Zn(OAc)2·2H2O, H3PO4, N,N'-dimethylpiperazine, and ethylene glycol or H2O (multiautoclave, 180 °C, 60 h). As revealed by single crystal XRD, [C6H16 N2]·[Zn2(HPO4)3]
crystallizes in the monoclinic space group P21/n with Z = 4. It is composed of tetrahedral units forming an open-framework with intersecting eight-membered ring channels.
— (SONG, Y.; YU*, J.; LI, Y.; ZHANG, M.; XU, R.; Eur. J. Inorg. Chem. 2004, 18,
3718-3723; State Key Lab. Inorg. Synth. Prep. Chem., Coll. Chem., Jilin Univ.,
Changchun 130023, Peop. Rep. China; Eng.) — W. Pewestorf
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