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2004
Dithiane derivatives
R 0490
Xanthates Derived from 1,3-Dithiane and Its Monosulfoxide; One-Carbon RadiEquivalents. — In contrast to the xanthate (III) the monosulfoxide (VI) is found to
50- 118 cal
be a useful equivalent of both formyl and methyl radicals. It smoothly undergoes radical
addition to a wide range of alkenes under mild, neutral conditions that are compatible
with most functional groups. Hydrolysis or reduction of these adducts allows formation
of several aldehydes or methylated products. — (DE GREEF, M.; ZARD*, S. Z.;
Tetrahedron 60 (2004) 35, 7781-7791; Lab. Synth. Org., CNRS, DCSO, Ec. Polytech.,
F-91128 Palaiseau, Fr.; Eng.) — Jannicke
2004
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