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2004
Molybdenum
I 5600
[C5H14N2][(MoO 3)3(SO4)]·H2O: Sulfated α-Molybdena Chains. — Title compound
(II) is characterized by single-crystal XRD (orthorhombic, space group P212121, Z = 4)
52- 019 and
IR spectroscopy. One-dimensional [(MoO3)3(SO4 )]2n n- chains, based on a neutral
α-molybdena backbone, are connected through an extensive hydrogen-bonding network containing the piperazinium cations and occluded water molecules. The direction
of the hydrogen bonding is primarily dictated by the nucleophilicity of the respective
oxide ligands, as determined using bond valence sums. — (GUTNICK, J. R.;
MULLER, E. A.; NARDUCCI SARJEANT, A.; NORQUIST*, A. J.; Inorg. Chem.
43 (2004) 21, 6528-6530; Dep. Chem., Haverford Coll., Haverford, PA 19041, USA;
Eng.) — Schramke
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