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2004
Tungsten
I 5700
52- 020
Synthesis and Electrochemistry of the Monolacunary Dawson-Type Tungstoarsenate [H4AsW17O61]11- and Some First-Row Transition-Metal Ion Derivatives.
— The title compounds are characterized by elemental analysis, IR and UV/VIS spectroscopy and representative examples by 183W NMR spectroscopy. Several experiments
indicate that the substitution occurs in the α2 position. Substituted compounds are characterized by cyclic voltammetry. The electrocatalytic properties of all compounds are
illustrated by the reduction of nitrite by reduced [H4AsW18O62]7- and of nitrate by reduced α2-[(H2O)Cu(H 4AsW17O61)]9-. — (MBOMEKALLE, I.-M.; KEITA, B.; LU, Y.
W.; NADJO*, L.; CONTANT, R.; BELAI, N.; POPE, M. T.; Eur. J. Inorg. Chem.
2004, 20, 4132-4139; Lab. Chim. Phys., CNRS, Univ. Paris-Sud,
F-91405 Orsay, Fr.; Eng.) — W. Pewestorf
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