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2004
Cyclopentane derivatives
Q 0030
Catalytic Intermolecular Pauson—Khand-Type Reaction: Strong Directing
of Pyridylsilyl and Pyrimidylsilyl Groups and Isolation of Ru Complexes
52- 059 Effect
Relevant to Catalytic Reaction. — A detailed investigation of the recently published
[2 + 2 + 1] cycloaddition of alkenyl(2-pyridyl)silanes, alkynes and carbon monoxide
in the presence of Ru3(CO)12 is presented. During this study new removable directing
groups are discovered and catalytically active ruthenium complexes [cf. (VII), (VIII)]
are isolated. — (ITAMI*, K.; MITSUDO, K.; FUJITA, K.; OHASHI, Y.; YOSHIDA*,
J.-I.; J. Am. Chem. Soc. 126 (2004) 35, 11058-11066; Dep. Synth. Chem. Biol Chem.,
Grad. Sch. Eng., Kyoto Univ., Nishikyo, Kyoto 615, Japan; Eng.) — Nuesgen
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