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2005
Structure
D 2000
02- 007
Synthesis and Structure of [C3N2H5][Cu(H2PO4)2Cl]·H2O with a Chain Structure:
The First Example of an Organically Templated Copper(II) Phosphate. — Light
blue long needle like crystals of the title compound are synthesized by evaporating a
MeCN solution of CuCl2·2H2O, imidazole, and H3PO4 at room temperature for 2—3 d.
The compound crystallizes in the monoclinic space group P21/n with Z = 4 (single crystal XRD). The structure is the first example of an organically templated copper(II)
phosphate and contains copper chlorophosphate chains which are topologically similar
to those observed in fornacite and vauquelinite. — (NEERAJ, S.; LOISEAU, T.;
RAO, C. N. R.; CHEETHAM*, A. K.; Solid State Sci. 6 (2004) 10, 1169-1173; Dep.
Mater., Univ. Calif., Santa Barbara, CA 93106, USA; Eng.) — W. Pewestorf
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