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2005
Structure
D 2000
04- 005
The Rediscovery of Alfred Werner's Second Hexol. ?
A compound originally prepared by Alfred Werner but structurally misassigned is
shown by three independent X-ray structural analyses to be a hexanuclear species
which can now be regarded as Werner's second hexol. The dark green compound
[Co6(OH)8O2(NH3)14](ZnCl 4)2(Zn(OH2)Cl 3)2�2O crystallizes in the triclinic space
group P1 with Z = 2 (single crystal XRD). The compound is further characterized by
1
H NMR spectroscopy. [Co 6(OH) 8(O) 2(NH3)14](NO3)6�2O crystallizes in the monoclinic space group P21/n with Z = 2. ? (JACKSON, W. G.; MCKEON, J. A.;
ZEHNDER*, M.; NEUBERGER, M.; FALLAB, S.; Chem. Commun. (Cambridge)
2004, 20, 2322-2323; Inst. Anorg. Chem., Univ. Basel, CH-4056 Basel, Switz.; Eng.)
? W. Pewestorf
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