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2005
Carboxylic acid esters
P 0360
Simple Access to 2-Methylalk-2-enoates and Insect Pheromones by Zinc-PromotReduction of Baylis—Hillman-Derived Allylic Bromides. — A versatile method
04- 072 ed
for the efficient and highly stereoselective preparation of (E)-2-methylacrylates (III) by
reduction of 2-(bromoamethyl)alkanoates (II) derived from Baylis—Hillman adducts
(I) using Zn-acetic acid is developed and successfully applied to the synthesis of the
male ant pheromone (IV). — (FERNANDES, L.; BORTOLUZZI, A. J.; SA*, M. M.;
Tetrahedron 60 (2004) 44, 9983-9989; Dep. Quim., Univ. Fed. Santa Catarina, 88049
Florianopolis, Santa Catarina, Brazil; Eng.) — H. Toeppel
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