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2005
Molybdenum
I 5600
Syntheses and Crystal Structures of the Compounds In3.7Mo15S19, In 1.6Rb2Mo15S19,
In2.2CsMo15S19 and ScTl 2Mo 15S19 Containing Mo6 and Mo9 Clusters. — The new
06- 024 title
compounds are synthesized by solid state reactions in sealed Mo crucibles at about
1250 °C using MoS2, In2S3, Rb2MoS4, Cs2MoS4, Sc2S3, Tl2S, and Mo as starting materials. As revealed by single crystal XRD, the four compounds crystallize in the hexagonal space group P63/m with Z = 2. The Mo—S framework of these compounds consists of an equal mixture of Mo6S8S6 and Mo9S11S6 cluster units which are interconnected through Mo—S bonds. — (SALLOUM, D.; GOUGEON*, P.; ROISNEL, T.;
POTEL, M.; J. Alloys Compd. 383 (2004) 1-2, 57-62; Lab. Chim. Solide Inorg. Mol.,
CNRS, Univ. Rennes, F-35042 Rennes, Fr.; Eng.) — W. Pewestorf
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