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2005
Peptides
U 0400
06- 176
An Efficient Synthetic Route to Glycoamino Acid Building Blocks for Glycopeptide Synthesis. — A short (three-step) synthetic route from unprotected sugar (I) to
glycosylated asparagine building blocks such as (III) and (IV) for glycopeptide synthesis includes microwave-assisted Kochetkov amination as a key reaction. This route is
also applied to di- and oligosaccharides and yields glycosylated asparagine building
blocks in a short period of time with minimal work-up. — (BEJUGAM, M.;
FLITSCH*, S. L.; Org. Lett. 6 (2004) 22, 4001-4004; Dep. Chem., Univ. Edinburgh,
Edinburgh EH9 3JJ, UK; Eng.) — Steudel
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