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2005
Niobium
I 5100
08- 017
Octahedral Metal Clusters as Building Units in a Neutral Layered Honeycomb
Network, [Zn(en)]2[Nb6Cl 12(CN)6]. — The structures of the title compound (V) and
its precursor (III) are determined by single crystal XRD. (III) crystallizes in the tetragonal space group I41/amd with Z = 4 and compound (V) in the trigonal space group
P3 with Z = 1. The structure of (V) consists of neutral layers built of octahedral
[Nb6Cl 12]2+ cluster units and [Zn(en)]2+ groups linked by cyanide ligands. —
(YAN, B.; DAY, C. S.; LACHGAR*, A.; Chem. Commun. (Cambridge) 2004, 21,
2390-2391; Dep. Chem., Wake Forest Univ., Winston-Salem, NC 27109, USA; Eng.)
— W. Pewestorf
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