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2005
Tungsten
I 5700
08- 020
Isolation and Molecular Structure of a Monomeric, Tris[peroxotitanium(IV)]-Substituted α-Dawson Polyoxometalate Derived from the Tetrameric Anhydride
Form Composed of Four Tris[titanium(IV)]-Substituted α-Dawson Substructures
and Four Bridging Titanium(IV) Octahedral Groups. — Compound (II) is characterized by TG/DTA, FTIR, and solution (31 P and 183W) NMR spectroscopy. As revealed
by single crystal XRD it crystallizes in the monoclinic space group P21/c with Z = 4.
Compound (II) exhibits η2-coordination of the peroxo group to the Ti(IV) atom. —
(SAKAI, Y.; KITAKOGA, Y.; HAYASHI, K.; YOZA, K.; NOMIYA*, K.; Eur. J.
Inorg. Chem. 2004, 23, 4646-4652; Dep. Chem., Kanagawa Univ., Kanagawa 259-12,
Japan; Eng.) — W. Pewestorf
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