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2005
Halogenation
O 0235
An Insight of the Reactions of Amines with Trichloroisocyanuric Acid. —
reaction between amines and TCCA leads to dichloroamines, e.g. (II), whereas
08- 049 The
amino acids, e.g. (VI), undergo decarboxylation to give nitriles. Secondary stereocenters keep unchanged cf. (IX). If the reaction is performed as one-pot procedure, the
use of dichloromethane results in no yield, so dimethylformamide is used instead. —
(DE LUCA, L.; GIACOMELLI, G.; Synlett 2004, 12, 2180-2184; Dip. Chim., Univ.
Sassari, I-07100 Sassari, Italy; Eng.) — C. Oppel
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