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2005
Uranium
I 5900
09- 020
[N(CH2CH 2NH3)3][U3O2F13]·2H2O: A Novel Organically Templated Mixed-Valent
Uranium Oxyfluoride with a Hybrid Network Structure. — The novel mixed-valent uranium oxyfluoride (II) crystallizes in the monoclinic space group P21 with
Z = 2 (single crystal XRD). The inorganic network consists of [U2F10]2- sheets formed
by corner- and edge-sharing UIVF9 tricapped trigonal prisms and [UO2F3]- chains constructed from edge-sharing UVIO2F5 pentagonal bipyramids. The organic cations and
water molecules are located between the sheets. Magnetic susceptibility measurements
confirm the oxidation state of the uranium ions. — (WANG, C.-M.; LIAO, C.-H.; LIN,
H.-M.; LII*, K.-H.; Inorg. Chem. 43 (2004) 26, 8239-8241; Inst. Chem., Acad. Sin.,
Taipei 115, Taiwan; Eng.) — Schramke
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