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2005
Alcohols
Q 0230
09- 063
Highly Diastereo- and Enantioselective Reagents for Aldehyde Crotylation. —
The cis- and trans-crotylsilane reagents (I) and (III) are developed and used in highly
enantioselective syn- and anti-selective aldehyde crotylation reactions. The reagents
are easily prepared in bulk and are storable crystalline solids, the crotylation reactions
are experimentally trivial, and the chiral diamine controller may be easily recovered in
high yield. — (HACKMAN, B. M.; LOMBARDI, P. J.; LEIGHTON*, J. L.; Org.
Lett. 6 (2004) 23, 4375-4377; Dep. Chem., Columbia Univ., New York, NY 10027,
USA; Eng.) — Steudel
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