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2005
Carbohydrates
U 0500
Synthesis of Antitumor Phosphatidylinositol Analogues from Glucose by the Use
Ring-Closing Olefin Metathesis. — The synthesis of three novel phosphatidylino10- 193 of
sitols (VIII), which have promising anti-tumor activity is described. Key steps of the
synthesis are a zinc-mediated fragmentation of (I), a vinyl Grignard addition and a
ring-closing metathesis in order to convert the carbohydrate into the carbocycle (VI),
which is the key intermediate in the synthesis of (VIII). — (ANDRESEN, T. L.;
SKYTTE, D. M.; MADSEN*, R.; Org. Biomol. Chem. 2 (2004) 20, 2951-2957; Dep.
Chem., Tech. Univ. Den., DK-2800 Lyngby, Den.; Eng.) — Bartels
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