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2005
Biochemical syntheses
O 0035
High-Efficiency and Minimum-Waste Continuous Kinetic Resolution of Racemic
by Using Lipase in Supercritical Carbon Dioxide. — A novel continuous12- 040 Alcohols
-flow supercritical carbon dioxide process for kinetic resolution of racemic alcohols (I)
is performed with an immobilized lipase to lead to a quantitative mixture of the corresponding optically active acetates (III) and unreacted alcohols (IV) with up to 99% e.e.
in both cases. — (MATSUDA*, T.; WATANABE, K.; HARADA, T.; NAKAMURA,
K.; ARITA, Y.; MISUMI, Y.; ICHIKAWA, S.; IKARIYA, T.; Chem. Commun.
(Cambridge) 2004, 20, 2286-2287; Dep. Mater. Chem., Ryukoku Univ., Otsu, Shiga
520, Japan; Eng.) — M. Paetzel
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