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2005
Oxazole derivatives
R 0220
An Environmentally Friendly α-Hydroxyallylation Reaction of the Garner Aldehyde: A Comparative Assessment of Alternative Barbier Conditions. — An opti13- 134 mization
study of the title reaction of aldehyde (I) with acetate (II) in terms of chemical
yield, stereochemistry, and overall time by use of either zinc or indium metal, and three
different types of reaction media is presented. The results obtained under the different
conditions are assessed with a view to stereoselectivity, economic and mass
efficiency, and environmental compatibility. — (LOMBARDO*, M.; GIANOTTI, K.;
LICCIULLI, S.; TROMBINI, C.; Tetrahedron 60 (2004) 51, 11725-11732; Dip.
Chim. "G. Ciamician", Univ. Bologna, I-40126 Bologna, Italy; Eng.) — Klein
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