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2005
Nickel
I 7300
14- 024
2The closo-Pb210 Zintl Ion in the [Ni@Pb10] Cluster. — The structure of compound (III) (yield given in gram) is prepared by single crystal XRD (monoclinic, space
group C2/c). The title anion has virtual D4d point symmetry and consists of a
closo-Pb210 bicapped square antiprism centered by a Ni atom. Compound (III) is further characterized by 207Pb NMR and laser desorption/ionization time-of-flight MS.
The [Ni@Pb12]2- anion of byproduct (IV) is isostructural with the [Pt@Pb12]2- anion.
— (ESENTURK, E. N.; FETTINGER, J.; EICHHORN*, B.; Chem. Commun.
(Cambridge) 2005, 2, 247-249; Dep. Chem. Biochem., Univ. Md., College Park,
MD 20742, USA; Eng.) — Schramke
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