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2005
Ketones
Q 0350
14- 087
Influence of Catalytic System Composition on Formation of Adamantane Containing Ketones. — Treatment of acyl chlorides with Grignard reagents in the presence
of AlCl3/CuCl(1:1) offers a new, efficient, cheap, and fast approach to unsymmetrical
ketones including those with adamantyl residue. Alcoholic side products are not formed
under these conditions. Composition of the catalytic system and time of addition of
Grignard reagent have an important influence on the yield of the ketone and the formation of side products. — (VICHA, R.; POTACEK*, M.; Tetrahedron 61 (2005) 1,
83-88; Dep. Org. Chem., Fac. Sci., Masaryk Univ., CZ-611 37 Brno, Czech Republic;
Eng.) — Jannicke
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