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2005
Carbohydrates
U 0500
Synthesis of a Useful Lauryl Thioglycoside of Sialic Acid and Its Application. —
title compound is readily prepared from ester (I) and 1-dodecanethiol and isolated
15- 186 The
as a mixture of isomers (III) and (VII). Its reactivity with some alcohols under conditions A) is investigated. Generally, the β-isomer (III) gives a higher yield of the products. Furthermore, (III) is transformed to the azide (VIII) which reacts with cyclohexanol to give the known glycoside (IX)/(X). — (MATSUOKA*, K.; ONAGA, T.;
MORI, T.; SAKAMOTO, J.-I.; KOYAMA, T.; SAKAIRI, N.; HATANO, K.;
TERUNUMA, D.; Tetrahedron Lett. 45 (2004) 51, 9383-9386; Dep. Funct. Mater.
Sci. Eng., Fac. Eng., Saitama Univ., Urawa, Saitama 338, Japan; Eng.) — Lindner
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