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2005
Molybdenum
I 5600
Hydrothermal Synthesis and Structures of the Homoleptic Iodate Complexes
23)6] (M: Mo, Zr). — The compounds (III) and (VI) crystallize in the trigonal
20- 025 [M(IO
space group R3 with Z = 3 (single crystal XRD). The compounds consist of alkali metal
cations and isolated [A(IO3)6]2- (A: Mo, Zr) anions with Mo and Zr in the +4 oxidation
state. This is the first evidence for the stabilization of MoIV by iodate. The compounds
may also provide molecular precursors to extended structures containing octahedral
transition metal iodate units. — (SHEHEE, T. C.; PEHLER, S. F.;
ALBRECHT-SCHMITT*, T. E.; J. Alloys Compd. 388 (2005) 2, 225-229; Dep.
Chem., Auburn Univ., Auburn, AL 36849, USA; Eng.) — W. Pewestorf
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