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2005
Organo-silicon compounds
S 0060
The Three-Component Joining Reaction of Primary Amines, Electron-Deficient
Olefins, and α-Halogen-Substituted Allylsilanes Catalyzed by Copper(I) Chlo20- 177 ride.
— The title method affords tertiary amines bearing three different substituents. It
proceeds with high yields for most of the aliphatic amines, but is unsuccessful for
anilines. The sterically demanding amines (XIb) and (XIc) give the products in low
yields. This fact can be circumvented by decrease of the amount of chloroacetone. —
(KOZUKA*, M.; INOUE, A.; TSUCHIDA, T.; MITANI, M.; Synlett 2004, 15,
2756-2760; Dep. Chem. Mater. Eng., Fac. Eng., Shinshu Univ., Wakasato, Nagano 380,
Japan; Eng.) — Steudel
2005
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