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2005
Reactions of organo-metal compounds
O 0350
Preparation of Cyclic Alkenylmagnesium Reagents via an Iodine/Magnesium
— The reaction of various cyclic alkenyl iodides with iPrMgCl x LiCl pro21- 069 Exchange.
duces the corresponding alkenylmagnesium reagents. After reaction with a series of
electrophiles the expected products are isolated in 53—91% yield. Remarkably, the
mild reaction conditions of the I/Mg-exchange tolerate the presence of sensitive diene
functionalities. — (REN, H.; KRASOVSKIY, A.; KNOCHEL*, P.; Chem. Commun.
(Cambridge) 2005, 4, 543-545; Fachbereich Chem., Ludwig-Maximilians-Univ.,
D-81377 Muenchen, Germany; Eng.) — M. Paetzel
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