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2005
Organo-phosphorus compounds
S 0080
Carbon—Carbon Bond Formation by Cyclization of Dienes Using PhosphoRadicals in Water. — Carbocyclic and heterocyclic compounds with
22- 177 rus-Centered
phosphorus functionalities are synthesized by radical cyclization of dienes in water.
Best results are achieved by adding cetyltrimethylammonium bromide as surfactant to
improve the solubility of diphenylphosphine oxide in water. For the hydrophobic diene
(V) satisfactory yield is accomplished performing the reaction in dioxane in the presence of tBu-O-O-tBu. — (CHO, D. H.; JANG*, D. O.; Synlett 2005, 1, 59-62; Dep.
Chem., Yonsei Univ., Wonju 220-710, S. Korea; Eng.) — S. Adam
2005
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