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2005
Cobalt
I 7200
23- 023
V
Octacyanometallate-Based Single-Molecule Magnets: C oII
9 M 6 (M: W, Mo). ?
Dark-red single crystals of [Co9{W(CN)8}6(MeOH)24]�H2O and
[Co 9{Mo(CN)8}6(MeOH)24 ]�eOH�H2O are synthesized by reaction of
CoCl2�2O with Na3[M(CN)]8� 2O (M: W, Mo) in MeOH solutions, below 20 癈 in
the dark for several days. As revealed by single crystal XRD, both compounds crystallize in the monoclinic space group C2/c with Z = 2. Magnetic measurements indicate
that both compounds behave as single-molecule magnets. ? (SONG*, Y.; ZHANG,
P.; REN, X.-M.; SHEN, X.-F.; LI, Y.-Z.; YOU, X.-Z.; J. Am. Chem. Soc. 127 (2005)
11, 3708-3709; Coord. Chem. Inst., Nanjing Univ., Nanjing 210093, Peop. Rep. China;
Eng.) ? W. Pewestorf
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