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2005
Nickel
I 7300
23- 025
First Nickel(II) Cation Inclusion within the Mixed-Valence Polyoxomolybdate
Capped with Four NiII(en)(H2O) Groups: Hydrothermal Synthesis and Structure
of [MoV8 MoVI
O30(µ2-OH)6(NiIIO4){Ni II(en)(H 2O)}4]. — Title compound (III),
4
which can also be formulated as H6[Ni{Ni(en)(H2O)}4Mo12O40], crystallizes in the
monoclinic space group C2/m with Z = 4 (single crystal XRD). The structure shows a
central ε-Keggin core centered by Ni, in which four Ni(en)(H 2O) groups replace four
facial MoO3 units. — (CUI, X.-B.; ZHENG, S.-T.; YANG*, G.-Y.; Z. Anorg. Allg.
Chem. 631 (2005) 4, 642-644; State Key Lab. Struct. Chem., Fujian Inst. Res. Struct.
Matter, Chin. Acad. Sci., Fujian, Fuzhou 350002, Peop. Rep. China; Eng.) —
Schramke
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