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2005
Cycloaddition reactions
O 0070
Evaluation of Ethyl 2-Carbomethoxyethenesulfinates as 2-Hydroxymethyl EneEquivalents in the Diels—Alder Reaction. — Both dienophiles (I) and (V) act
23- 039 thiol
as masked 2-hydroxymethyl enethiol equivalents in Diels—Alder cycloaddition reactions with various dienes followed by reduction of the resulting cycloadducts. The latter
are obtained as mixtures of sulfur epimers which are unified in the subsequent reduction
step. Under the appropriate reaction conditions, simultaneous reduction of both the sulfinate and the carboxylate ester functionalities occurs (to be continued). —
(FARAGHER, R. J.; ALBERICO, D.; SCHWAN*, A. L.; Tetrahedron 61 (2005) 5,
1115-pp; Guelph-Waterloo Cent. Grad. Work Chem., Dep. Chem. Biochem., Univ.
Guelph, Guelph, Ont. N1G 2W1, Can.; Eng.) — Klein
2005
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