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2005
Tungsten
I 5700
26- 016
Crystallographic Studies of a Molybdenum-Rich Diarsenotungstate and Reaction
of FeIII with Its Isomerically Pure α1- and α2-Monolacunary Derivatives. — As
revealed by single crystal XRD, K2Na4[α-As2Mo6W12O62]0.5[α-As2W18O62]0.5·11H2O
crystallizes in the triclinic space group P1 with Z = 2. Isomerically pure α1-(VII) and
α2-(VIII) are synthesized by reaction of Fe III with the lacunary α1- and α2-precursors
(III) and (V), respectively. Complexes (VII), (VIII), and their lacunary precursors (III)
and (V) are clearly distinguishable by cyclic voltammetry. — (MBOMEKALLE, I.
M.; LU, Y. W.; KEITA, B.; NADJO*, L.; NEIWERT, W. A.; HARDCASTLE, K. I.;
HILL, C. L.; ANDERSON, T. M.; Eur. J. Inorg. Chem. 2005, 8, 1547-1551; Lab.
Chim. Phys., CNRS, Univ. Paris-Sud, F-91405 Orsay, Fr.; Eng.) — W. Pewestorf
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