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2005
Hydrolysis
O 0050
27- 035
Effects of Counter Cations in Selective Monohydrolyses of Symmetric Diesters.
— The monohydrolysis of diesters (I) and (III) is studied. Whereas the monoester (II)
can be prepared from (I) in nearly quantitative yield, different hydroxides yield various
ratios of (IV):(V) in the case of diester (III). It is shown that more reactive bases show
higher selectivities, with KOH yielding the highest selectivity. — (NIWAYAMA*, S.;
RIMKUS, A.; Bull. Chem. Soc. Jpn. 78 (2005) 3, 498-500; Dep. Chem., Okla. State
Univ., Stillwater, OK 74078, USA; Eng.) — M. Bohle
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