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2005
Oxocarboxylic acids and esters
P 0290
Ti-Crossed-Claisen Condensation Between Carboxylic Esters and Acid Chlorides
Acids: A Highly Selective and General Method for the Preparation of Various
30- 053 or
β-Keto Esters. — The title procedure can also be performed by a new protocol: the
sodium salts of the acids are transformed with trichloroacetyl chloride into mixed anhydrides which react with the carboxylic esters. Both methods are applied to the syntheses of muscone (XXII) and (Z)-jasmone (XXV). — (MISAKI, T.; NAGASE, R.;
MATSUMOTO, K.; TANABE*, Y.; J. Am. Chem. Soc. 127 (2005) 9, p2854-p2855;
Dep. Chem., Sch. Sci. Technol., Kwansei Gakuin Univ., Sanda, Hyogo 669, Japan;
Eng.) — Klein
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