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2005
Reduction
O 0220
32- 059
Reduction of Alkyl and Vinyl Sulfonates Using the CuCl2·2H2O—Li—DTBB(cat.)
System. — The system efficiently reduces triflates and mesylates to the corresponding
hydrocarbons under very mild reaction conditions. Enol and dienol triflates are reduced
to alkenes and dienes, respectively. No over-reduction is detected even using an excess
of agent or long reaction times. With CuCl2·D2O, deuterium-labeled alkanes and alkenes can be prepared in a simple and economic way. — (RADIVOY*, G.; ALONSO,
F.; MOGLIE, Y.; VITALE, C.; YUS, M.; Tetrahedron 61 (2005) 15, 3859-3864; Dep.
Quim., Univ. Nac. Sur, 8000 Bahia Blanca, Argent.; Eng.) — Klein
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