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2005
Aldehyde derivatives
P 0190
The Novel and Efficient Direct Synthesis of N,O-Acetal Compounds Using a HyIodine(III) Reagent: An Improved Synthetic Method for a Key Inter34- 078 pervalent
mediate of Discorhabdins. — The oxidative fragmentation of α-amino alcohols (I)
and α-amino acids (VI) in the presence of a hypervalent iodine compound allows the
direct synthesis of N,O-acetals (III) and (VII), respectively. This method is used to develope an improved synthesis of the key intermediate (V) of discorhabdins. —
(HARAYAMA, Y.; YOSHIDA, M.; KAMIMURA, D.; KITA*, Y.; Chem. Commun.
(Cambridge) 2005, 13, 1764-1766; Grad. Sch. Pharm. Sci., Osaka Univ., Suita,
Osaka 565, Japan; Eng.) — M. Paetzel
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