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2005
Copper
I 7400
35- 026
Copper(I) Hexafluoroantimonate — An Example of a Compound with CuI in a
Solely Fluorine Environment. — CuSbF6 is prepared by reaction of excess Cu0 with
SbF5 in anhydrous HF (25 °C, 2 weeks) and by reduction of Cu(SbF 6)2 with Cu in anhydrous HF (25 °C, 4 d; ≈50% yield). CuSbF6 crystallizes in the rhombohedral space
group R3 with Z = 3 (single crystal XRD) and is isostructural with LiSbF 6. The structure consists of isolated layers of regular [SbF6]- octahedra and Cu + ions. —
(MAZEJ*, Z.; BENKIC, P.; J. Fluorine Chem. 126 (2005) 5, 803-808; Dep. Inorg.
Chem. Technol., Jozef Stefan Inst., 1000 Ljubljana, Slovenia; Eng.) — Schramke
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