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2005
Structure
D 2000
37- 008
Crystal Structure of Rubidium Tetraiodothallate(III) Dihydrate, RbTlI4�2O.
? Single crystals of the title compound are grown by addition of I2 to an equimolar
mixture of TlI, RbI, and 18-crown-6 in CH2Cl2/EtOH solution. RbTlI4� 2O crystallizes in the cubic space group Fm3c with Z = 4. The structure is characterized by an
ReO3 analogous arrangement of Rb centered [TlI4] tetrahedra. The cuboctahedral
cavities of this structure are filled with water molecules and additional disordered
Rb+ cations. ? (RIEGER, F.; MUDRING*, A.-V.; Z. Anorg. Allg. Chem. 631 (2005)
9, 1571-1573; Inst. Anorg. Chem., Univ. Koeln, D-50939 Koeln, Germany; Eng.) ?
Schramke
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