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2005
Halogenation
O 0235
Electrochemical Partial Fluorination of α,β-Unsaturated Ketones. — Anodic
of α,β-unsaturated ketones (I) using ammonium fluorides as supporting
37- 042 fluorination
electrolytes and fluorine sources at room temperature yields the expected vicinal difluoroketones as mixtures of two diastereomers. However, anodic fluorination of hindered phenol-containing chalcone (IV) yields only the two monofluorinated compounds (V) and (VI). — (DINOIU*, V.; KANNO, K.; Rev. Roum. Chim. 49 (2004)
12, 989-993; Nenitzescu Inst. Org. Chem., Roum. Acad., RO-77208 Bucharest, Rom.;
Eng.) — C. Hettrich
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