вход по аккаунту


Патент USA US3086774

код для вставки
April 23, 1963
Filed April 18, 1961
3 Sheets-Sheet 1
April 23, 1963
Filed April 18, 1961
:5 Sheets-Sheet 2
April 23, 1963
Filed April 18, 1961
3 Sheets-Sheet 3
execute two or more successive heat treatments using
different gases, with the furnace adapted to provide pre
cise control of gas ?ow, whereby the materials or articles
being treated are fully contacted with the treating gases
While the gases are prevented from reacting with each
Jacob Howard Beck, 44 Varick Hill Road, Newton, Mass.
Filed Apr. 18, 1961, Ser- No. 163,881
12 Claims. (Cl. 263-8)
This invention relates to heat treating furnaces and more
particularly to a novel furnace construction especially
adapted to carry out two successive and distinct heat treat
ing operations without interruption of production.
other in the muf?e and also from migrating.
A further speci?c object of the present invention is to
provide a tandem furnace which includes two or more
separate heat-treating sections in which heat treating gases
10 are introduced and caused to contact articles moving
The present invention is a direct outgrowth of the cur
through the furnace, with mobile baffle means provided
to assure full gas coverage of each article at a speci?c
rent epoch of miniaturization of electronic and electro
time and temperature.
mechanical components. In the manufacture of such de
Another speci?c object of the present invention is to
vices as transistors, photo-diodes, miniature relays, and
provide a tandem furnace comprising two or more suc
micro-switches, controlled heating is used to establish,
cessive heat-treating sections, each ?lled with a different
modify, eliminate, or stabilize various physical and/or
active gas, and an intermediate neutralizing gas section
chemical characteristics. Thus, for example, heating may
I etween each pair of heat-treating sections, said inter
be used to assure formation of strong surface-to-surface
bonds and high-pressure hermetic seals.
Heretofore there has been available various batch- and
continuous-type furnaces which could be used with com
plete success to execute one-stage heat treating processes,
as, for example, a simple reduction process, or multi
stage heat treating processes where the time interval and 25
space between separate stages is not critical. However,
a problem has existed where the heat testing process
comprises two or more immediately successive heat-treat
ing stages with each stage utilizing a diiferent atmosphere.
The latter situation requires a furnace wherein the various
heat-treating steps may be executed in rapid succession
without interruption of production and without removal
of the heat treated materials or articles until the heat
treating process has been completed fully. Heretofore,
mediate section having a gas which functions as a ?uid
barrier to prevent migration of active gas from one heat
treating section to another heat-treating section.
Other objects and many of the attendant advantages of
the present invention will become readily apparent from
a study of the following detailed speci?cation when con
sidered together with the accompanying drawings wherein:
FIG. 1 is a side elevation of a tandem furnace embody
the present invention;
FIG. 2 is a schematic longitudinal section of the mu?ie
embodied in the furnace of FIG. 1;
FIG. 3 is an enlarged fragmentary longitudinal section
illustrating the ?ow of gases through the mui?e;
FIG. 4 is an enlarged perspective view of a typical type
of ‘conveyor employable in the apparatus of FIGS. 1-3;
FIG. 5 is a cross-sectional view of a mu?le using a ?rst
such multi-stage processes could be executed on a batch 35
type of mobile ba?le;
basis, but at a relatively low production rate and at the
FIG. 6 is a view similar to FIG. 5 but illustrating a
expense of elaborate gas-handling mechanism. Prior ef
forts to provide a high production furnace with various
second type of mobile ba?le;
stages have not been successful for various reasons, chief
of which are the problems of isolating the gases in the
?ed mu?ie; and
di?erent stages and attaining good gas diffusion in each
stage. Prevention of migration of gas from one stage
to another may be necessary to avoid formation of an
explosive or gas mixture, to assure completion of the
desired treatment, or to maintain proper temperature
gradients between successive stages. Good gas diffusion
and separation is essential in order to attain proper treat
ment of each article or piece of material at a given stage
in the furnace. The usual approach to a solution of
FIG. 7 is a fragmentary longitudinal section of a modi
FIG. 8 is a cross-sectional view of the muffle of FIG. 7.
Referring now to FIG. '1, there is shown a tandem
furnace embodying the present invention.
This illus
trated embodiment is designed to execute a speci?c two
stage heat treatment on special electronic parts. In the
first stage, reduction and decarburization is effected by
means of hydrogen gas, and in the second stage oxida
tion is effected by means of oxygen gas. However, it
is to be understood that the furnace may be adapted to
these problems is to provide a plurality of stationary 50 execute other processes without departing from the prin
ciples of the present invention. The illustrated furnace
gas barriers and ba?les within the oven. However, gas
comprises a muffle identi?ed generally at 2 through which
barriers and baffles alone have been inadequate-they
articles to be treated are transported by an endless con
tend to retard the ?ow of gas through the oven, causing
veyor belt 4 that is driven by a conventional drive sys
it to collect in some locations while flowing freely in
tem which is shown in part at 6. Articles may be fed
others. To overcome this, high gas velocities have been 55
onto and removed from the conveyor by hand or by an
used. However, these high gas velocities have inhibited
material handling equipment. The upstream and
rather than improved the diffusion and separation of the
ends of the mu?le are ?tted with enlarged
gases. Accordingly, it often has been necessary to ex
terminal sections 8 and 10, respectively, which prefera
tend the furnace length in order to assure proper di?usion
bly are provided with vertically slidable doors 12 and
and separation and assure proper contact of the treat 60 14. These doors permit the inlet and outlet openings
ing gases with the materials being treated. This intro
of the mu?le to be adjusted in size. In practice, they
duces other problems, including higher costs, more critical
are made just large enough to allow passage of the ar
heat control, and complicated construction. It also re
ticles undergoing treatment. A major part of the mu?le
quired rapid transfer of materials which in many cases
65 is encased in an insulated heating cabinet 18. Conven
is not desirable.
tional electrical heating elements (not shown) are dis
Accordingly, the primary object of the present inven
posed in cabinet 18 in close surrounding relation to the
tion is to provide a tandem furnace which is free of the
mu?ie, whereby to ef?ciently heat the muffle to the de
limitations and disadvantages of furnaces heretofore avail
sired temperatures. The heating elements may be dis
able for executing two or more heat-treating procedures
70 posed uniformly along the muf?e; on the other hand,
on materials and objects.
they may be arranged in discrete groups so as to cause
A more speci?c object of the present invention is to
different portions of the mut?e to be heated to ditferent
provide a tandem furnace which is especially adapted to
temperatures, A water jacket 20 functions to keep the
downstream end of the mu?le relatively cool, whereby
to cool the treated articles as they pass out of the mu?le.
A control panel identi?ed generally at 22a and 22b in
cludesv recording instruments in addition to controls for
thewconveyor, belt, the heating elements, and the gases
which: are supplied' to the rnu?tle.
The internal construction and the cross-sectional con
?guration of themuf?e will now be described with ref
sections 62 and 66, and, the horizontal portion includes
the remaining sections 70, 68, and 64. The reason for
the inclined portion is to improve ?ow of hydrogen gas
in section 66. The hydrogengas tends to ?ow upward
and the inclined section assists this normal ?ow, thereby
helping to prevent back?ow into the end section 62,
The nitrogen, which is introduced via pipes 74 and
76, effectively vforms a curtain which also helps to pre
vent air from moving into the rnu?le and also to prevent
erence particularly to FIGURES 2, 3, 5, and 6; The 10 hydrogen gas from ?owing out of the upstream end‘ of
the mu?le. Similarly, the nitrogen which is introduced
lel, vertically extending side walls 30 and 32, a hori
via pipes 78 and 80 forms a curtain which prevents air
zontal bottom wall 34, and two inwardly inclined top
from moving into the mu?le and also prevents oxygen
wall sections 36and 368. Disposed within the mu?le
‘from ?owingout of the downstream end of the muf?e.
mu?leis of ?ve-sided construction, comprising two paral
and extending along its length are two perforated parti 15 Small baf?es 99 help establish the nitrogen curtains. The
tion plates 40 and 42. The partition plate 40 is gen
nitrogen which is introduced via pipe 94 vfunctions to
erally described as the “?oorj? while the partition plate
prevent the hydrogen gas from mixing with the’ oxygen
42 is generally described as the “ceiling.” The space
gas. In this manner, thepqualityyof the gases in the
disposed, between the bottom wall 34 and the floor 40
mu?le is effectively controlled while the danger of ex
is generally described as the “basement.” This passage 20 plosive mixtures ?owing ‘out of the mu?le into the sur
way, is identi?ed generallyat 44. The passageway 46
rounding work area is eliminated. The major portion of
between the ceiling plate 42 and the two inclined top
the oxygen flows out of the mufHe through pipe 92‘.
plates 36, and ,38 is ‘generally described as the “attic”
To the extent already described, the ?ow of gases within
or “upside down gutter” of the ba?ie. The ends of the
the mu?le is as follows: Nitrogen ‘introduced through
mu?le are, provided with end plates 48 and 56 which 25 the pipes 74 and 76 ?ows up throughvthe ?oor 4Q and
have rectangular openings 52a and 5212 respectively. A
down through the ceiling 42. Most of the nitrogen tends
plurality of ?xed vertical ba?le plates 54, 56, 58, and
to flow out of the inlet end of the mui?ewhilethe re
:60 also are secured within the mu?le. These ba?les have
mainder of the nitrogen tends to ?ow downstream along
like openings 52c-f corresponding to openings 52a and
the basement, the gutter, and also the central portion
52b. As illustrated in FIG. 2, the ba?le 54 is mounted 30 of the mu?le toward the hydrogen section '66. The
nearest to the endplate 48 and demarcates therewith
amount of nitrogenwhich ?ows into the section 66 is
a relatively short end section 62. The fourth ba?le 60
is located nearest to the opposite end plate 50 and de
relatively small. The hydrogen which is introduced
through the pipe 84 tends to ?ow up through the ?oor
marcates therewith a relatively short end section 64. The
40 into the central portion of the mu?le and then up
second and third ba?les 56 and 58 are spaced to de?ne 35 through the ceiling 42 into the gutter 46. > At the same
two relatively long sections 66 and 68 and an intermedi
ate shorter section 70. The upper end of ba?le 56 is
time, the general ?ow of the hydrogen is in a down
direction. However, due to the absence of bat?es
provided with one or more openings 72.
within section 66, a substantial portion of the hydrogen
L'Ihree dilferent gases-—-nitrogen, hydrogen, and oxy 40 tends to immediately reach the, gutter section» 66 instead
gen—are supplied to the mu?le. As stated previously,
of ?owing downstream along the central portion of the
the hydrogen causes reduction and decarburization while
the oxygen produces controlled oxidation of the arti
In this connection, ‘it is to be observed that the con
cles being treated. The purpose of the nitrogen is to
veyor 4 must have a plurality of openings so as to allow
provide a neutralizing atmosphere which prevents forma
the gas to pass ‘from the basement to the gutter. A satis
tion of an explosive mixture by preventing undesired mi 45 tactory type of endless conveyor is formed of metallic
gration of the hydrogen and oxygen. The manner in
links. This type of conveyor belt is illustrated in FIG.
which this is done is explained hereafter.
4, the links being identi?ed generally at 100. The ad
Referring now to FIGS. 1 and 2, nitrogen gas is sup
plied to the upstream end section 62 of the mu?le via
vantage of an articulated metal conveyor belt is that it
is strong and will withstand elevated temperatures while
pipes 74 and 76. Nitrogen is also supplied to the down 50 at the same time allowing easy passage therethrough of
stream end section 64 via pipes 78 and '80. Although
not shown, it is to be understood that the pipes 74, 76,
The oxygen gas flows into section 68 through the pipe
90 and tends to ?ow immediately toward the outlet pipe
voir via automatically controlled valves.
92. Some oxygen tries to ?ow, upstream but is pre
Hydrogen is admitted to the long upstream section 66 55 vented from doing so freely by the nitrogen gas in the
via a pipe 84 and is removed ‘from that section _via
intermediate section 70. No oxygen can reach the hy
a second pipe 86. ‘Pipe 86 extends up from the muf?e
drogen section 66. Only a little oxygen reaches the end
and, as shown in FIG. 1, is provided at its free end
section 64, and this is blocked by the nitrogen introduced
with a hydrogen igniter and. burn-off. unit 88. This ig
through the pipes 78 and 80. As a result, substantially
niter and burn-01f unit is of conventional construction
all of the oxygen introduced via pipe 90 is con?ned within
and iswell known to persons skilled in the art. Accord~
the oxidation stage.
78, and 80 are connected to a suitable nitrogen reser
ingly, no claim is made to the hydrogen igniter and bum
o? unit per se.
Oxygen is supplied to the long downstream section 68
via a pipe 90 and is removed via a second ‘pipe 92.
An additional pipe 94 is connected to the intermedi
ate section 70. Nitrogen is introduced to the mu?le via
pipe ‘94 and ‘is removed mainly by pipe 86. The open
ings 72 in lb'a?le 56 facilitate removal of the nitrogen
To the extent heretofore ‘described, the furnace is capa
ble of heat treating articles at a relatively rapid rate.
65 However, due to the fact that the hydrogen and oxygen
gases tend to ?ow directly from the inlet pipes’ to the
outlet pipes instead of di?using evenly within the heat
treating sections 66 and 68, not all of the articles on the
conveyor may be fully contacted by the gases, and as a
result, the reduction or oxidation treatment may be in
‘gas. Although as shown in FIG. 2 the mu?le may be 70
‘a straight unit, it is preferred to make it angular in length
as shown in FIG. 1 with an inclined portion generally
V g
This di?iculty is obviated by the use of moving ba?les
which cause the gases ?owing from the inlet pipes to the
identi?ed at 2a and a horizontal portion generally identi
outlet pipes to be channeled alongside individual articles
tied at 2b. The inclined portion includes the ?rst two 75 on the conveyor, thereby diffusing the gas fully within
the treatment chamber so as to contact all of the articles
uniformly. These battles are of two forms. 'One form
is illustrated in FIGS. 3 and 5; the second form is illus
trated in FIGS. 2 and 6.
Referring now to FIGS. 3 and 5, the moving ba?ies
may consist of metallic plates 110 which are ?xed to
the conveyor 4 at ?xed intervals. These plates 110- are
viding a continuous open-ended passageway of 'prede
termined minimum cross-section, means for introducing
a continuous ?ow of gas to the interior of said passage
way at one point and removing said gas at another point,
means for providing gaseous curtains at either end of
said passageway for isolating said gas from the outer
atmosphere, a continuous perforated web conveyor pass
ing through said passageway, and a plurality of trans
versely extending baf?e elements on said conveyor for
sized to just pass through the openings 52a-f which are
formed in the end plates 43 and 50 and the baffle plates
channeling said gas vertically around individual articles
54-60. The spacing between these moving baf?e plates 10 to be treated disposed on said conveyor, said ba?ie ele
is determined by the size of the articles to be treated.
ments sized to substantially ?ll said passageway at the
Generally, the smaller the articles to be treated, the nar
rower the spacing between ba?ie plates 110. These ba?les
minimum cross section thereof, whereby to hinder migra
tion of gas longitudinally of said passageway.
actually serve a second function. They periodically
2. A furnace comprising an elongate unitary mu?le
block the openings in the ?xed baffles 544%, thereby
adapted to be heated and providing an elongated open
assisting in prevention of migration of gases between ad
ended passageway of predetermined minimum cross
jacent treatment sections and helping in removal of gases
section, means for introducing a continuous flow of a
through pipes 86 and 92.
?rst gas to the interior of said passageway at a ?rst pre
The articles to be treated may be placed directly on
determined location, means for introducing a continuous
the conveyor 4, as shown, for example, in FIGS. 3 and 5
flow of a second gas to the interior of said passageway
where articles A are disposed on the conveyor between the
at a second predetermined location, means for providing a
adjacent plates 110. Alternatively, the articles may be
gaseous curtain in said passage between said two pre
supported in small holders, commonly called “boats.”
determined locations, whereby to isolate said ?rst gas
It is to be noted that the mobile ba?ie plates need not
from said second gas, a continuous web conveyor passing
be physically attached to the conveyor. Instead, they
through said passageway, said conveyor having openings
may be attached to or formed integral with the boats in
therein through which said gases may ?ow vertically, and
which the articles to be treated are supported. This
a plurality of imperforate ba?le elements on said con
variation is illustrated in FIGS. 2 and 6 where articles 13
veyor for channeling said gases vertically around articles
are supported in boats 116 to each of which is secured
disposed on said conveyor, whereby to fully contact said
a flat metallic baffle plate 118 (sometimes called a “sail”).
articles with said gases, said baf?e elements having an
One advantage of this variation is that the spacing of
outline which substantially fully ?lls said passageway at
the battle plates is not ?xed. Another advantage of this
points of said minimum cross-section.
variation is that the conveyor can follow a tortuous path
3. A furnace as de?ned by claim 2 wherein said battle
as in FIG. 1 instead of being mounted as in FIG. 2 so
elements are physically attached to said conveyor.
that one surface thereof never engages a drive pulley or 35
4. A furnace as de?ned by claim 2 wherein said ba?ie
a guide pulley.
elements are attached to holders for articles to be treated.
The mu?ie construction need not be exactly as illus
5. A furnace as de?ned by claim 4 wherein said article
trated in FIGS. 2, 3, 5, and 6, but can be varied. One
holders are removable from said conveyor.
important modi?cation is illustrated in FIGS. 7 and 8.
'6. A furnace comprising an elongated unitary mu?le
The mu?’ie construction 2A shown in these ?gures is 40 adapted to be heated and provided with ?rst and second
essentially the same as the one illustrated in FIGS. 2,
3, 5, and 6, except that the ceiling plate 42 is omitted.
Substituted for the ceiling plate is a series of transversely
parallel perforated longitudinally extending plates sub
dividing its interior into ‘(1) a central main passageway,
(2.) a bottom passageway, and (3) a top passageway,
extending ba-?ie plates 124 whose ends are secured to
means subdividing said bottom and top passageways into
the vertical side walls 3% and 32a. Ba?ie plates 124
a like number of compartments, means for introducing a
are inclined, the direction of inclination depending upon
?rst gas into a ?rst one of said bottom compartments and
the direction of gas flow which is required. Thus, in
for removing it from a corresponding ?rst one of said top
FIG. 7, some of the ba?ie plates 124 are inclined left
compartments, means for introducing a second gas into
to right so as to direct gas downstream toward an outlet
pipe 125 and other baf?e plates 124 are inclined right to
left to direct gas flow upstream toward an outlet pipe
128. The upper edges of bai?e plates v124 collectively
function to demarcate the “attic” dda of the mu?le. In
this construction additional vertical ‘baffles 139 may be
utilized to demarcate separate compartments. Like the
baf?es 54-60 of FIG. 2, ba?les 13% have openings through
a second one of said bottom compartments and for remov
ing it from a corresponding second one of said top com
partments, means for introducing a third gas into a third
one of said bottom compartments located intermediate
said ?rst and second bottom compartments and for remov
ing said third gas from a corresponding third top com
partment located intermediate said ?rst and second top
compartments, whereby said ?rst and second gases will
which the articles and the supporting conveyor can pass.
pass from said ?rst and second bottom compartments to
These openings are identi?ed generaly at 132.
said ?rst and second top compartments respectively
The advantage of the construction of FIGS. 7 and 8
through said central passageway with said third gas isolat
resides in the fact that it avoids the need for a perforated
ing said ?rst gas from said second gas.
ceiling plate, thereby cutting down both weight and cost.
7. A furnace as de?ned by claim 6 further including an
Obviously, many modi?cations and variations of the
endless conveyor extending through said central passage
present invention are possible in the light of the above
way, said conveyor having a series of perforations through
teachings. For example, the overall length of an oven
which said gases may pass, whereby articles mounted on
embodying the present invention can be varied as desired. 65 said conveyor will be exposed to and contacted by said
Similarly, the number of processing stages may be varied
?rst and second gases as said articles are transported
according to the process to be carried out. It is to be
through said central passageway.
understood, therefore, that the invention is not limited in
8. A furnace as de?ned by claim 7 further including a
its application to the details of construction and arrange
plurality of transversely-extending ba?ie elements disposed
ment of parts speci?cally described or illustrated, and that
on said conveyor, said baffle elements sized to just pass
within the scope of the appended claims it may be prac
through said central passageway and spaced from each
ticed otherwise than as speci?cally described or illustrated.
other so as to channel said gases vertically around articles
I claim:
disposed on said conveyor, whereby to fully contact said
1. A furnace for heat treating articles comprising,
with said gases.
an elongate unitary muffle adapted to be heated and pro 75
'9. Apparatus for heating articles ?rst in' a reducing‘ at
mosphere and (then in an oxidizing atmosphere comprising
and bottom passageways into ?ve manifold sections, means
for introducing nitrogen gas into the ?rst and last of the
a unitary elongate mu?ie adapted to be heated and pro—
top and bottom manifold sections, whereby to provide an
viding a continuous open-ended passageway, said passage
isolating gaseous curtain for said‘ centralpassage'way at
way having a ?rst inclined portion and a second horizon
both ends thereof, means for introducing a continuous
tal portion, means forming a ?rst elongated open-ended
?ow of hydrogen gas to the second bottom manifold sec
gas chamber in said inclined portion of said passageway,
tion and for removing said hydrogen gas from the second
means forming a second elongated open-ended gas cham
top manifold section, means for introducing oxygen gas
ber in the horizontal portion of said passageway, a perfo
into the fourth bottom manifold section and for removing
rated partition de?ning a gas distributing channel in each 10
said oxygen gas from the fourth top manifold section,
of said gas chambers, a perforated partition de?ning a gas
and means for introducing a third gas into thetthird bot
collecting channel in each of said gas chambers, means
tom manifold section and for removing said third gas
for establishing a continuous flow of hydrogen gas in said
from the third top manifold section, the gas in said third
?rst chamber, means for establishing a continuous flow of
sections effectively preventing mixing of said oxygen and
oxygen gas in said second chamber, and means providing 15 hydrogen gases in said central passageway.
a gaseous curtain between said two chambers whereby
12. Apparatus as de?ned by claim 11 further including
the gas in one chamber is prevented from migrating into
an endless article conveyor mounted to travel through
the other chamber.
said central passageway, and individual ba?ie elements on
10. Apparatus as de?ned by claim 9 further including
conveyor for channeling said hydrogen, and oxygen
individual mobile ba?ie elements within said open-ended
gases around individual articles disposed on said conveyor,
passageway for channeling said gases around articles
whereby to fully contact said articles with said gases.
traveling through said passageway, whereby to fully con
tact said articles with said gases.
References Cited in the ?le of this patent
11. A mu?ie for use in subjecting individual articles to
heat treatment ?rst in a reducing atmosphere and there 25
after in an oxidizing atmosphere comprising, an elongated
Dreyfoos ____________ __ July 26, 1921
unitary structure open at both ends, a pair of elongated
Dretfein _____________ __ Oct. v28, 1930
perforated plates disposed within said structure at the (top
Cope _______________ __ June 15, 1937
and bottom thereof and subdividing said structure into a
?rst top passageway, a second central passageway, and
a third bottom passageway, means ‘subdividing said top
Schmidt et a]. ________ __ Feb. 27, 1951
Gilbert ______________ __ Feb. 8, 1955
Без категории
Размер файла
771 Кб
Пожаловаться на содержимое документа